Crystallography Open Database

Information card for entry 4075712

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Structure parameters

Formula	C32 H56 Mg N2 O2 Si2
Calculated formula	C32 H56 Mg N2 O2 Si2
SMILES	[Mg](N([Si](C)(C)C)c1c(cc(cc1C)C)C)(N([Si](C)(C)C)c1c(cc(cc1C)C)C)([O]1CCCC1)[O]1CCCC1
Title of publication	Synthesis and Structural Characterization of Magnesium Amide Complexes Containing −N[(R)(SiMe3)] Ligands
Authors of publication	Tang, Yongjun; Zakharov, Lev N.; Rheingold, Arnold L.; Kemp, Richard A.
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	5
Pages of publication	836
a	13.4473 ± 0.0008 Å
b	16.0187 ± 0.0009 Å
c	16.3754 ± 0.0009 Å
α	90°
β	101.875 ± 0.001°
γ	90°
Cell volume	3451.9 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0576
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1165
Weighted residual factors for all reflections included in the refinement	0.121
Goodness-of-fit parameter for all reflections included in the refinement	1.158
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301830 (current)	2025-08-20	Add cross-references to PubChem compounds in COD range 4/07/ Each referenced PubChem compound corresponds to the full crystal structure.	4075712.cif
178646	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/57.	4075712.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075712.cif
50633	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075710, 4075711, 4075712, 4075713, 4075714, 4075715, 4075716, 4075717, 4075718 via cif-deposit CGI script.	4075712.cif