Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4075715
Preview
| Coordinates | 4075715.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C32 H60 Mg N6 Si2 |
|---|---|
| Calculated formula | C32 H60 Mg N6 Si2 |
| SMILES | C1(CCCCC1)N([Si](C)(C)C)[Mg](N(C1CCCCC1)[Si](C)(C)C)([n]1ccc(N(C)C)cc1)[n]1ccc(N(C)C)cc1 |
| Title of publication | Synthesis and Structural Characterization of Magnesium Amide Complexes Containing −N[(R)(SiMe3)] Ligands |
| Authors of publication | Tang, Yongjun; Zakharov, Lev N.; Rheingold, Arnold L.; Kemp, Richard A. |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 5 |
| Pages of publication | 836 |
| a | 10.4814 ± 0.0019 Å |
| b | 18.532 ± 0.003 Å |
| c | 18.641 ± 0.003 Å |
| α | 90° |
| β | 94.469 ± 0.003° |
| γ | 90° |
| Cell volume | 3609.8 ± 1.1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0558 |
| Residual factor for significantly intense reflections | 0.0429 |
| Weighted residual factors for significantly intense reflections | 0.1101 |
| Weighted residual factors for all reflections included in the refinement | 0.1181 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301830 (current) | 2025-08-20 | Add cross-references to PubChem compounds in COD range 4/07/ Each referenced PubChem compound corresponds to the full crystal structure. |
4075715.cif |
| 178646 | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/57. |
4075715.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4075715.cif |
| 50633 | 2012-03-31 | ../uploads/cif-deposit/cod/cif Adding structures of 4075710, 4075711, 4075712, 4075713, 4075714, 4075715, 4075716, 4075717, 4075718 via cif-deposit CGI script. |
4075715.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.