Crystallography Open Database

Information card for entry 4075730

Preview

Coordinates	4075730.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H68 Cl N O P2 Pd
Calculated formula	C50 H68 Cl N O P2 Pd
Title of publication	Catalytic Suzuki Coupling Reactions by Amido Phosphine Complexes of Palladium
Authors of publication	Liang, Lan-Chang; Chien, Pin-Shu; Huang, Mei-Hui
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	3
Pages of publication	353
a	10.26 ± 0.0002 Å
b	12.804 ± 0.0002 Å
c	19.634 ± 0.0003 Å
α	71.302 ± 0.001°
β	87.086 ± 0.001°
γ	70.073 ± 0.001°
Cell volume	2291.94 ± 0.07 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0506
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.1009
Weighted residual factors for all reflections included in the refinement	0.1267
Goodness-of-fit parameter for all reflections included in the refinement	1.259
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178646 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/57.	4075730.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075730.cif
50639	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075730 via cif-deposit CGI script.	4075730.cif