Crystallography Open Database

Information card for entry 4075812

Preview

Coordinates	4075812.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H36 N2 S2 Si2 Zn
Calculated formula	C20 H36 N2 S2 Si2 Zn
Title of publication	Coordination Complexes of Zinc with Reactive ESiMe3(E = S, Se, Te) Ligands
Authors of publication	DeGroot, Marty W.; Corrigan, John F.
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3378
a	9.9388 ± 0.0002 Å
b	17.7413 ± 0.0004 Å
c	15.1322 ± 0.0004 Å
α	90°
β	94.876 ± 0.0011°
γ	90°
Cell volume	2658.56 ± 0.11 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1075
Residual factor for significantly intense reflections	0.0455
Weighted residual factors for significantly intense reflections	0.0916
Weighted residual factors for all reflections included in the refinement	0.1073
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178647 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/58.	4075812.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075812.cif
50679	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075811, 4075812, 4075813, 4075814 via cif-deposit CGI script.	4075812.cif