Crystallography Open Database

Information card for entry 4075833

Preview

Coordinates	4075833.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H33 N2 P Pb Si2
Calculated formula	C24 H33 N2 P Pb Si2
SMILES	C1=c2ccccn2[Pb](N([Si](C)(C)C)[Si](C)(C)C)[P]1(c1ccccc1)c1ccccc1
Title of publication	A Heterotopically Chelated Low-Valent Lead Amide1
Authors of publication	Murso, Alexander; Straka, Michal; Kaupp, Martin; Bertermann, Rüdiger; Stalke, Dietmar
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3576
a	8.5944 ± 0.0015 Å
b	17.482 ± 0.003 Å
c	18.411 ± 0.003 Å
α	102.425 ± 0.003°
β	96.536 ± 0.003°
γ	95.131 ± 0.003°
Cell volume	2665.3 ± 0.8 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0206
Residual factor for significantly intense reflections	0.0179
Weighted residual factors for significantly intense reflections	0.0405
Weighted residual factors for all reflections included in the refinement	0.0412
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178647 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/58.	4075833.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075833.cif
50693	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075833 via cif-deposit CGI script.	4075833.cif