Crystallography Open Database

Information card for entry 4075890

Preview

Coordinates	4075890.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35.5 H52 Cl Mn2 O11 P3 Sn
Calculated formula	C35.5 H52 Cl Mn2 O11 P3 Sn
Title of publication	Phosphonate−Stannylene Coupling in the Reactions of the Anion [Mn2{μ-OP(OEt)2}{μ-P(OEt)2}(CO)6]2-with SnR2Cl2(R = Bu, Ph)
Authors of publication	Liu, Xiang-Yang; Ruiz, Miguel A.; Lanfranchi, Maurizio; Tiripicchio, Antonio
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3527
a	12.367 ± 0.004 Å
b	20.625 ± 0.005 Å
c	35.067 ± 0.007 Å
α	90°
β	91.24 ± 0.02°
γ	90°
Cell volume	8942 ± 4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1332
Residual factor for significantly intense reflections	0.0669
Weighted residual factors for significantly intense reflections	0.181
Weighted residual factors for all reflections included in the refinement	0.2217
Goodness-of-fit parameter for all reflections included in the refinement	1.153
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4075890.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075890.cif
50727	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075890 via cif-deposit CGI script.	4075890.cif