Crystallography Open Database

Information card for entry 4076107

Preview

Coordinates	4076107.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C11 H20 B5 Rh S
Calculated formula	C11 H20 B5 Rh S
Title of publication	Heteronuclear Tungsten and Cobalt Derivatives of the 16-Electron Half-Sandwich Complex Cp*Rh[E2C2(B10H10)] (E = S, Se)
Authors of publication	Cai, Shuyi; Jin, Guo-Xin
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	22
Pages of publication	5280
a	18.071 ± 0.003 Å
b	12.41 ± 0.002 Å
c	15.353 ± 0.003 Å
α	90°
β	114.356 ± 0.003°
γ	90°
Cell volume	3136.6 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0659
Residual factor for significantly intense reflections	0.0433
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.1076
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178650 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/61.	4076107.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4076107.cif
50846	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4076107 via cif-deposit CGI script.	4076107.cif