Crystallography Open Database

Information card for entry 4076366

Preview

Coordinates	4076366.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H32 Cl N3 Si2 Sn
Calculated formula	C21 H32 Cl N3 Si2 Sn
SMILES	[Sn]1(Cl)[N](c2ccc(cc2)C)=C(N([Si](C)(C)C)[Si](C)(C)C)N1c1ccc(cc1)C
Title of publication	Addition of Lappert's Stannylenes to Carbodiimides, Providing a New Class of Tin(II) Guanidinates
Authors of publication	Chlupatý, Tomáš; Padělková, Zdeňka; DeProft, Frank; Willem, Rudolph; Růžička, Aleš
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	6
Pages of publication	2203
a	9.964 ± 0.0005 Å
b	11.0551 ± 0.0005 Å
c	13.6129 ± 0.0005 Å
α	68.42 ± 0.003°
β	77.555 ± 0.003°
γ	68.335 ± 0.004°
Cell volume	1290.37 ± 0.11 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0276
Residual factor for significantly intense reflections	0.0223
Weighted residual factors for significantly intense reflections	0.0504
Weighted residual factors for all reflections included in the refinement	0.0538
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178652 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/63.	4076366.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4076366.cif
51937	2012-04-07	../uploads/cif-deposit/cod/cif Adding structures of 4076365, 4076366, 4076367, 4076368, 4076369 via cif-deposit CGI script.	4076366.cif