Crystallography Open Database

Information card for entry 4076374

Preview

Coordinates	4076374.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63.75 H60.5 Ge O3 P4 Rh
Calculated formula	C63.75 H51 Ge O3 P4 Rh
Title of publication	Synthesis and Reactivity of Rhodium Complexes Bearing [E(o-C6H4PPh2)3]-Type Tetradentate Ligands (E = Si, Ge, and Sn)
Authors of publication	Kameo, Hajime; Ishii, Sho; Nakazawa, Hiroshi
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	6
Pages of publication	2212
a	24.2964 ± 0.0009 Å
b	24.2266 ± 0.0007 Å
c	39.8765 ± 0.0016 Å
α	90°
β	106.537 ± 0.0015°
γ	90°
Cell volume	22501.2 ± 1.4 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0695
Residual factor for significantly intense reflections	0.0629
Weighted residual factors for significantly intense reflections	0.1385
Weighted residual factors for all reflections included in the refinement	0.1415
Goodness-of-fit parameter for all reflections included in the refinement	1.232
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4076374.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4076374.cif
51938	2012-04-07	../uploads/cif-deposit/cod/cif Adding structures of 4076370, 4076371, 4076372, 4076373, 4076374 via cif-deposit CGI script.	4076374.cif