Crystallography Open Database

Information card for entry 4076632

Preview

Coordinates	4076632.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57 H44 Cl4 Co2 O4 P4
Calculated formula	C57 H44 Cl4 Co2 O4 P4
Title of publication	Bis(diphenylphosphino)acetylene as Bifunctional Ligand in Dicobalt Carbonyl Complexes
Authors of publication	Hong, Fung-E; Chang,; Chang, Ruei-E; Chen, Shu-Chun; Ko, Bao-Tsan
Journal of publication	Organometallics
Year of publication	2002
Journal volume	21
Journal issue	5
Pages of publication	961
a	11.8168 ± 0.0008 Å
b	12.8713 ± 0.0008 Å
c	36.274 ± 0.002 Å
α	90°
β	96.236 ± 0.001°
γ	90°
Cell volume	5484.5 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0667
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.1617
Weighted residual factors for all reflections included in the refinement	0.1709
Goodness-of-fit parameter for all reflections included in the refinement	1.225
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178655 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/66.	4076632.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4076632.cif
54011	2012-04-20	cif/ Adding structures of 4076632, 4076633, 4076634, 4076635, 4076636 via cif-deposit CGI script.	4076632.cif