Crystallography Open Database

Information card for entry 4077328

Preview

Coordinates	4077328.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65.5 H50 Cl N2 O5 P4 Ru2
Calculated formula	C65.5 H50 Cl N2 O5 P4 Ru2
Title of publication	Synthesis and Reactivity of a Diruthenium Diazoalkane Complex
Authors of publication	Gao, Yuan; Jennings, Michael C.; Puddephatt, Richard J.; Jenkins, Hilary A.
Journal of publication	Organometallics
Year of publication	2001
Journal volume	20
Journal issue	16
Pages of publication	3500
a	15.293 ± 0.0012 Å
b	15.293 ± 0.0012 Å
c	27.764 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	6493.3 ± 0.9 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.2192
Residual factor for significantly intense reflections	0.078
Weighted residual factors for significantly intense reflections	0.1599
Weighted residual factors for all reflections included in the refinement	0.1952
Goodness-of-fit parameter for all reflections included in the refinement	0.927
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4077328.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4077328.cif
54295	2012-04-24	cif/ Adding structures of 4077327, 4077328, 4077329, 4077330 via cif-deposit CGI script.	4077328.cif