Crystallography Open Database

Information card for entry 4078022

Preview

Coordinates	4078022.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H120 La2 N6 O4 Si4
Calculated formula	C74 H104 La2 N6 O4 Si4
Title of publication	Synthesis and Characterization of Lanthanide Amides Bearing Aminophenoxy Ligands and Their Catalytic Activity for the Polymerization of Lactides
Authors of publication	Zhang, Jie; Qiu, Jinshui; Yao, Yingming; Zhang, Yong; Wang, Yaorong; Shen, Qi
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	8
Pages of publication	3138
a	10.0939 ± 0.0016 Å
b	14.244 ± 0.003 Å
c	15.441 ± 0.003 Å
α	108.887 ± 0.003°
β	92.534 ± 0.003°
γ	101.661 ± 0.003°
Cell volume	2042.7 ± 0.7 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0555
Residual factor for significantly intense reflections	0.0476
Weighted residual factors for significantly intense reflections	0.1197
Weighted residual factors for all reflections included in the refinement	0.1246
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178669 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/80.	4078022.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4078022.cif
57671	2012-05-18	cif/ Adding structures of 4078017, 4078018, 4078019, 4078020, 4078021, 4078022, 4078023 via cif-deposit CGI script.	4078022.cif