Crystallography Open Database

Information card for entry 4078226

Preview

Coordinates	4078226.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H44 N2 O P2 S Si Sn
Calculated formula	C39 H44 N2 O P2 S Si Sn
Title of publication	Reactivity of a Tin(II) (Iminophosphinoyl)(thiophosphinoyl)methanediide Complex toward Isocyanates and Rhodium(I) Chloride
Authors of publication	Guo, Jia-Yi; Li, Yongxin; Ganguly, Rakesh; So, Cheuk-Wai
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	10
Pages of publication	3888
a	30.8813 ± 0.0011 Å
b	11.158 ± 0.0004 Å
c	22.3386 ± 0.0008 Å
α	90°
β	104.853 ± 0.002°
γ	90°
Cell volume	7440.1 ± 0.5 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0948
Residual factor for significantly intense reflections	0.0612
Weighted residual factors for significantly intense reflections	0.1625
Weighted residual factors for all reflections included in the refinement	0.1916
Goodness-of-fit parameter for all reflections included in the refinement	1.351
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178671 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/82.	4078226.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4078226.cif
59859	2012-06-14	cif/ Adding structures of 4078226, 4078227, 4078228 via cif-deposit CGI script.	4078226.cif