Crystallography Open Database

Information card for entry 4080118

Preview

Coordinates	4080118.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C91.67 H139.67 N6 O4.17 Yb2
Calculated formula	C91.6667 H139.667 N6 O4.16667 Yb2
Title of publication	Reactivity of Ytterbium(II) Hydride. Redox Reactions: Ytterbium(II) vs Hydrido Ligand. Metathesis of the Yb‒H Bond
Authors of publication	Basalov, Ivan V.; Lyubov, Dmitry M.; Fukin, Georgy K.; Cherkasov, Anton V.; Trifonov, Alexander A.
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	5
Pages of publication	1507
a	20.671 ± 0.002 Å
b	26.709 ± 0.003 Å
c	29.791 ± 0.003 Å
α	111.023 ± 0.002°
β	106.486 ± 0.003°
γ	97.723 ± 0.003°
Cell volume	14200 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.3462
Residual factor for significantly intense reflections	0.1105
Weighted residual factors for significantly intense reflections	0.1754
Weighted residual factors for all reflections included in the refinement	0.2314
Goodness-of-fit parameter for all reflections included in the refinement	0.823
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178690 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/01.	4080118.cif
76872	2013-03-21	cif/ Adding structures of 4080116, 4080117, 4080118, 4080119, 4080120 via cif-deposit CGI script.	4080118.cif