Crystallography Open Database

Information card for entry 4080120

Preview

Coordinates	4080120.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H73 N2 O Si2 Yb
Calculated formula	C41 H73 N2 O Si2 Yb
Title of publication	Reactivity of Ytterbium(II) Hydride. Redox Reactions: Ytterbium(II) vs Hydrido Ligand. Metathesis of the Yb‒H Bond
Authors of publication	Basalov, Ivan V.; Lyubov, Dmitry M.; Fukin, Georgy K.; Cherkasov, Anton V.; Trifonov, Alexander A.
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	5
Pages of publication	1507
a	11.9708 ± 0.0007 Å
b	13.2488 ± 0.0007 Å
c	27.7865 ± 0.0016 Å
α	90°
β	93.543 ± 0.001°
γ	90°
Cell volume	4398.5 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0384
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.0672
Weighted residual factors for all reflections included in the refinement	0.0702
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178690 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/01.	4080120.cif
76872	2013-03-21	cif/ Adding structures of 4080116, 4080117, 4080118, 4080119, 4080120 via cif-deposit CGI script.	4080120.cif