Crystallography Open Database

Information card for entry 4080472

Preview

Coordinates	4080472.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H87 Cl N6 Si4 Yb2
Calculated formula	C52 H87 Cl N6 Si4 Yb2
Title of publication	Unexpected C‒H Bond Activation Promoted by Bimetallic Lanthanide Amido Complexes Bearing a META-Phenylene-Bridged Bis(β-diketiminate) Ligand
Authors of publication	Sun, Song; Sun, Qiu; Zhao, Bei; Zhang, Yong; Shen, Qi; Yao, Yingming
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	6
Pages of publication	1876
a	11.4491 ± 0.001 Å
b	11.927 ± 0.0011 Å
c	24.1294 ± 0.0019 Å
α	92.904 ± 0.002°
β	92.422 ± 0.002°
γ	114.028 ± 0.002°
Cell volume	2998.4 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0646
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.1207
Weighted residual factors for all reflections included in the refinement	0.1315
Goodness-of-fit parameter for all reflections included in the refinement	1.097
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178693 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/04.	4080472.cif
85935	2013-05-07	cif/ Adding structures of 4080471, 4080472, 4080473, 4080474 via cif-deposit CGI script.	4080472.cif