Crystallography Open Database

Information card for entry 4080880

Preview

Coordinates	4080880.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Li4[(N(SiMe3)CH2CH2)2O]2
Formula	C20 H52 Li4 N4 O2 Si4
Calculated formula	C20 H52 Li4 N4 O2 Si4
SMILES	C1C[O]2CC[N]3([Si](C)(C)C)[Li]4[N]5(CC[O]64CC[N]([Si](C)(C)C)([Li]23)[Li]6[N]1([Si](C)(C)C)[Li]5)[Si](C)(C)C
Title of publication	Synthesis and Reactivity of Titanium Hydrazido Complexes Supported by Diamido-Ether Ligands
Authors of publication	Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	10
Pages of publication	3091
a	10.3235 ± 0.0002 Å
b	12.5522 ± 0.0003 Å
c	14.3656 ± 0.0004 Å
α	91.4334 ± 0.0009°
β	108.448 ± 0.001°
γ	110.347 ± 0.001°
Cell volume	1636.49 ± 0.07 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1209
Residual factor for significantly intense reflections	0.0673
Weighted residual factors for all reflections	0.0478
Weighted residual factors for significantly intense reflections	0.0342
Weighted residual factors for all reflections included in the refinement	0.0312
Goodness-of-fit parameter for all reflections included in the refinement	1.0539
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178697 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/08.	4080880.cif
87314	2013-07-14	cif/ Adding structures of 4080880, 4080881, 4080882, 4080883, 4080884, 4080885, 4080886, 4080887, 4080888, 4080889, 4080890, 4080891, 4080892, 4080893 via cif-deposit CGI script.	4080880.cif