Crystallography Open Database

Information card for entry 4080882

Preview

Coordinates	4080882.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Ti(N2O)(NNPh2)(py)2
Formula	C32 H46 N6 O Si2 Ti
Calculated formula	C32 H46 N6 O Si2 Ti
Title of publication	Synthesis and Reactivity of Titanium Hydrazido Complexes Supported by Diamido-Ether Ligands
Authors of publication	Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	10
Pages of publication	3091
a	10.1761 ± 0.0001 Å
b	18.8025 ± 0.0002 Å
c	29.2221 ± 0.0004 Å
α	103.809 ± 0.0005°
β	99.2816 ± 0.0005°
γ	99.0278 ± 0.0006°
Cell volume	5245.98 ± 0.11 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1744
Weighted residual factors for all reflections	0.1147
Weighted residual factors for all reflections included in the refinement	0.0618
Goodness-of-fit parameter for all reflections included in the refinement	1.1477
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4080882.cif
87314	2013-07-14	cif/ Adding structures of 4080880, 4080881, 4080882, 4080883, 4080884, 4080885, 4080886, 4080887, 4080888, 4080889, 4080890, 4080891, 4080892, 4080893 via cif-deposit CGI script.	4080882.cif