Crystallography Open Database

Information card for entry 4081071

Preview

Coordinates	4081071.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H57 N5 Si2 Sm
Calculated formula	C37 H57 N5 Si2 Sm
Title of publication	Novel Lanthanide Amides Incorporating Neutral Pyrrole Ligand in a Constrained Geometry Architecture: Synthesis, Characterization, Reaction, and Catalytic Activity
Authors of publication	Wang, Fenhua; Wang, Shaowu; Zhu, Xiancui; Zhou, Shuangliu; Miao, Hui; Gu, Xiaoxia; Wei, Yun; Yuan, Qingbing
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	14
Pages of publication	3920
a	10.6399 ± 0.0007 Å
b	13.2558 ± 0.0008 Å
c	15.8529 ± 0.001 Å
α	81.524 ± 0.001°
β	82.051 ± 0.001°
γ	67.121 ± 0.001°
Cell volume	2029.4 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0287
Residual factor for significantly intense reflections	0.025
Weighted residual factors for significantly intense reflections	0.0703
Weighted residual factors for all reflections included in the refinement	0.0731
Goodness-of-fit parameter for all reflections included in the refinement	1.089
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178699 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/10.	4081071.cif
87986	2013-08-27	cif/ Adding structures of 4081069, 4081070, 4081071, 4081072, 4081073, 4081074, 4081075 via cif-deposit CGI script.	4081071.cif