Crystallography Open Database

Information card for entry 4081787

Preview

Coordinates	4081787.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H58 Al F Ge N
Calculated formula	C33 H58 Al F Ge N
Title of publication	Cooperative Ge‒N Bond Activation in Hydrogallation Products of Alkynyl(diethylamino)germanes (Et2N)nGe(C≡CtBu)4‒n
Authors of publication	Uhl, Werner; Tannert, Jens; Layh, Marcus; Hepp, Alexander; Grimme, Stefan; Risthaus, Tobias
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	22
Pages of publication	6770
a	9.7221 ± 0.0018 Å
b	10.986 ± 0.002 Å
c	17.117 ± 0.003 Å
α	90.675 ± 0.005°
β	97.831 ± 0.005°
γ	98.747 ± 0.005°
Cell volume	1789.1 ± 0.6 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0304
Residual factor for significantly intense reflections	0.0279
Weighted residual factors for significantly intense reflections	0.0753
Weighted residual factors for all reflections included in the refinement	0.0771
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178706 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/17.	4081787.cif
91763	2013-12-13	cif/ Adding structures of 4081786, 4081787, 4081788, 4081789, 4081790, 4081791, 4081792 via cif-deposit CGI script.	4081787.cif