Crystallography Open Database

Information card for entry 4081958

4081957 << 4081958 >> 4081959

Preview

Coordinates	4081958.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C144 H264 Hf4 N12 P4
Calculated formula	C144 H264 Hf4 N12 P4
Title of publication	Preparation of New Olefin Polymerization Precatalysts by Facile Derivatization of Imino‒Enamido ZrMe3and HfMe3Complexes
Authors of publication	Klosin, Jerzy; Fontaine, Philip P.; Figueroa, Ruth; McCann, Scott D.; Mort, Darrek
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	21
Pages of publication	6488
a	17.5453 ± 0.0003 Å
b	21.5242 ± 0.0003 Å
c	21.805 ± 0.0003 Å
α	103.574 ± 0.001°
β	90.342 ± 0.001°
γ	106.745 ± 0.001°
Cell volume	7641.2 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0277
Residual factor for significantly intense reflections	0.0204
Weighted residual factors for significantly intense reflections	0.0442
Weighted residual factors for all reflections included in the refinement	0.0476
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178708 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/19.	4081958.cif
91819	2013-12-13	cif/ Adding structures of 4081956, 4081957, 4081958, 4081959, 4081960, 4081961, 4081962, 4081963 via cif-deposit CGI script.	4081958.cif