Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4082167
Preview
Coordinates | 4082167.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C51 H61 B2 Cl17 F8 Ir2 N2 P2 |
---|---|
Calculated formula | C51 H48.5 B2 Cl17 F8 Ir2 N2 P2 |
Title of publication | Configurational Isomerization of Dinuclear Iridium and Rhodium Complexes with a Series of NPPN Ligands, 2-PyCH2(Ph)P(CH2)nP(Ph)CH2-2-Py (Py = Pyridyl,n= 2‒4) |
Authors of publication | Nakajima, Takayuki; Fukushima, Yuki; Tsuji, Minori; Hamada, Naoko; Kure, Bunsho; Tanase, Tomoaki |
Journal of publication | Organometallics |
Year of publication | 2013 |
Journal volume | 32 |
Journal issue | 24 |
Pages of publication | 7470 |
a | 10.299 ± 0.004 Å |
b | 25.652 ± 0.01 Å |
c | 28.619 ± 0.012 Å |
α | 109.201 ± 0.008° |
β | 94.241 ± 0.008° |
γ | 90.45 ± 0.009° |
Cell volume | 7117 ± 5 Å3 |
Cell temperature | 153 K |
Ambient diffraction temperature | 153 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.0583 |
Weighted residual factors for all reflections included in the refinement | 0.1658 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
178710 (current) | 2016-03-21 | cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/21. |
4082167.cif |
92208 | 2014-01-12 | cif/ Adding structures of 4082164, 4082165, 4082166, 4082167, 4082168, 4082169, 4082170, 4082171, 4082172, 4082173 via cif-deposit CGI script. |
4082167.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.