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Information card for entry 4082237
Preview
| Coordinates | 4082237.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C49 H43 N O Si Ti |
|---|---|
| Calculated formula | C49 H39 N O Si Ti |
| Title of publication | Reaction of Titanacyclobutene‒Silacyclobutene Fused-Ring Complexes with Nitriles via Formal Insertion of the C‒N Triple Bond of Nitrile into the Silacyclobutene Ring |
| Authors of publication | Zhao, Jing; Zhang, Shaoguang; Zhang, Wen-Xiong; Xi, Zhenfeng |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 33 |
| Journal issue | 1 |
| Pages of publication | 8 |
| a | 16.2653 ± 0.0006 Å |
| b | 19.3916 ± 0.0006 Å |
| c | 24.776 ± 0.0008 Å |
| α | 90° |
| β | 104.915 ± 0.003° |
| γ | 90° |
| Cell volume | 7551.3 ± 0.5 Å3 |
| Cell temperature | 180 ± 2 K |
| Ambient diffraction temperature | 180.15 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0576 |
| Residual factor for significantly intense reflections | 0.0469 |
| Weighted residual factors for significantly intense reflections | 0.1209 |
| Weighted residual factors for all reflections included in the refinement | 0.1291 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178711 (current) | 2016-03-21 | cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/22. |
4082237.cif |
| 110578 | 2014-04-19 | cif/ Updating files of 4082237 Original log message: Adding full bibliography for ./tmp-cod-update-bibliographies-18343/cifs/4082237.cif. |
4082237.cif |
| 109780 | 2014-04-17 | cif/ (saulius@koala.ibt.lt) Restoring in bulk the COD CIFs that had their bibliographies update recently: svn merge -r109779:109651 . The problem was that: a) the COD deposition pipeline incorrectly folded some text fields; b) it removed last page number from some CIFs that had it before. An attempt to updated bibliographies will be repeated with corrected scripts. |
4082237.cif |
| 109775 | 2014-04-17 | cif/ Updating files of 4082237 Original log message: Adding full bibliography for ./tmp-cod-update-bibliographies-28993/cifs/4082237.cif. |
4082237.cif |
| 93853 | 2014-01-17 | cif/ Adding structures of 4082235, 4082236, 4082237 via cif-deposit CGI script. |
4082237.cif |
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