Crystallography Open Database

Information card for entry 4082650

Preview

Coordinates	4082650.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H69 Al2 F2 P
Calculated formula	C48 H69 Al2 F2 P
Title of publication	Al/P-Based Frustrated Lewis Pairs: Limitations of Their Synthesis by Hydroalumination and Formation of Dialkylaluminum Hydride Adducts
Authors of publication	Uhl, Werner; Appelt, Christian; Backs, Jana; Westenberg, Hauke; Wollschläger, Agnes; Tannert, Jens
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	5
Pages of publication	1212
a	10.4489 ± 0.0004 Å
b	11.5051 ± 0.0004 Å
c	19.7216 ± 0.0008 Å
α	99.739 ± 0.001°
β	93.186 ± 0.001°
γ	97.84 ± 0.001°
Cell volume	2307.31 ± 0.15 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0694
Residual factor for significantly intense reflections	0.0536
Weighted residual factors for significantly intense reflections	0.1383
Weighted residual factors for all reflections included in the refinement	0.1493
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178715 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/26.	4082650.cif
106755	2014-03-16	cif/ Adding structures of 4082650 via cif-deposit CGI script.	4082650.cif