Crystallography Open Database

Information card for entry 4082683

Preview

Coordinates	4082683.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H58 B4 Li2 O6
Calculated formula	C32 H58 B4 Li2 O6
Title of publication	High-Yield Syntheses and Reactivity Studies of 1,2-Diborylated and 1,2,4,5-Tetraborylated Benzenes
Authors of publication	Seven, Ömer; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	5
Pages of publication	1291
a	11.0407 ± 0.0008 Å
b	13.5559 ± 0.0011 Å
c	14.4597 ± 0.0011 Å
α	87.243 ± 0.006°
β	67.938 ± 0.006°
γ	67.074 ± 0.006°
Cell volume	1835 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0656
Residual factor for significantly intense reflections	0.0492
Weighted residual factors for significantly intense reflections	0.1203
Weighted residual factors for all reflections included in the refinement	0.1281
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178715 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/26.	4082683.cif
132087	2015-02-19	cif/ (antanas@koala.ibt.lt) Replacing '_chemical_name_systematic' tag values consisting ';' with '?'.	4082683.cif
106764	2014-03-16	cif/ Adding structures of 4082678, 4082679, 4082680, 4082681, 4082682, 4082683, 4082684, 4082685 via cif-deposit CGI script.	4082683.cif