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Information card for entry 4082926
Preview
| Coordinates | 4082926.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C77 H126 Al2 B2 Lu N4 |
|---|---|
| Calculated formula | C77 H126 Al2 B2 Lu N4 |
| Title of publication | Half-Sandwich Rare-Earth-Metal Alkylaluminate Complexes Bearing Peripheral Boryl Ligands |
| Authors of publication | Dettenrieder, Nicole; Hollfelder, Christoph O.; Jende, Lars N.; Maichle-Mössmer, Cäcilia; Anwander, Reiner |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 33 |
| Journal issue | 7 |
| Pages of publication | 1528 |
| a | 13.4966 ± 0.0003 Å |
| b | 18.6094 ± 0.0005 Å |
| c | 32.8876 ± 0.0009 Å |
| α | 82.408 ± 0.002° |
| β | 83.663 ± 0.001° |
| γ | 79.017 ± 0.002° |
| Cell volume | 8006.9 ± 0.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.059 |
| Residual factor for significantly intense reflections | 0.0423 |
| Weighted residual factors for significantly intense reflections | 0.1082 |
| Weighted residual factors for all reflections included in the refinement | 0.1148 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178718 (current) | 2016-03-21 | cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/29. |
4082926.cif |
| 109889 | 2014-04-17 | cif/ Updating files of 4082926 Original log message: Adding full bibliography for 4082926.cif. |
4082926.cif |
| 109780 | 2014-04-17 | cif/ (saulius@koala.ibt.lt) Restoring in bulk the COD CIFs that had their bibliographies update recently: svn merge -r109779:109651 . The problem was that: a) the COD deposition pipeline incorrectly folded some text fields; b) it removed last page number from some CIFs that had it before. An attempt to updated bibliographies will be repeated with corrected scripts. |
4082926.cif |
| 109760 | 2014-04-17 | cif/ Updating files of 4082926 Original log message: Adding full bibliography for ./tmp-cod-update-bibliographies-28993/cifs/4082926.cif. |
4082926.cif |
| 108701 | 2014-04-02 | cif/ Adding structures of 4082926 via cif-deposit CGI script. |
4082926.cif |
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Users of the data should acknowledge the original authors of the
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