Crystallography Open Database

Information card for entry 4083184

Preview

Coordinates	4083184.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H28 Cl P Sn
Calculated formula	C20 H28 Cl P Sn
SMILES	[Sn]1(Cl)([P](c2ccc3c4c(ccc1c24)CC3)(C(C)C)C(C)C)(C)C
Title of publication	Sterically Restricted Tin Phosphines, Stabilized by Weak Intramolecular Donor‒Acceptor Interactions
Authors of publication	Athukorala Arachchige, Kasun S.; Sanz Camacho, Paula; Ray, Matthew J.; Chalmers, Brian A.; Knight, Fergus R.; Ashbrook, Sharon E.; Bühl, Michael; Kilian, Petr; Slawin, Alexandra M. Z.; Woollins, J. Derek
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	10
Pages of publication	2424
a	10.0545 ± 0.0011 Å
b	11.7826 ± 0.0013 Å
c	18.088 ± 0.002 Å
α	90°
β	93.768 ± 0.004°
γ	90°
Cell volume	2138.2 ± 0.4 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0666
Weighted residual factors for all reflections included in the refinement	0.2082
Goodness-of-fit parameter for all reflections included in the refinement	0.892
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178720 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/31.	4083184.cif
115866	2014-06-05	cif/ Updating files of 4083182, 4083183, 4083184, 4083185 Original log message: Adding full bibliography for 4083182--4083185.cif.	4083184.cif
113248	2014-05-09	cif/ Adding structures of 4083182, 4083183, 4083184, 4083185 via cif-deposit CGI script.	4083184.cif