Crystallography Open Database

Information card for entry 4083214

Preview

Coordinates	4083214.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H20 Cl2 N8 Pd Si
Calculated formula	C28 H20 Cl2 N8 Pd Si
Title of publication	7-Azaindol-1-yl(organo)silanes and Their PdCl2Complexes: Pd-Capped Tetrahedral Silicon Coordination Spheres and Paddlewheels with a Pd‒Si Axis
Authors of publication	Wahlicht, Sven; Brendler, Erica; Heine, Thomas; Zhechkov, Lyuben; Wagler, Jörg
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	10
Pages of publication	2479
a	8.9934 ± 0.0008 Å
b	8.9934 ± 0.0008 Å
c	16.093 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	1301.6 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0646
Residual factor for significantly intense reflections	0.0439
Weighted residual factors for significantly intense reflections	0.0917
Weighted residual factors for all reflections included in the refinement	0.0994
Goodness-of-fit parameter for all reflections included in the refinement	1.107
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4083214.cif
115879	2014-06-05	cif/ Updating files of 4083204, 4083205, 4083206, 4083207, 4083208, 4083209, 4083210, 4083211, 4083212, 4083213, 4083214, 4083215, 4083216 Original log message: Adding full bibliography for 4083204--4083216.cif.	4083214.cif
113611	2014-05-13	cif/ Adding structures of 4083204, 4083205, 4083206, 4083207, 4083208, 4083209, 4083210, 4083211, 4083212, 4083213, 4083214, 4083215, 4083216 via cif-deposit CGI script.	4083214.cif