Crystallography Open Database

Information card for entry 4083282

Preview

Coordinates	4083282.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C149 H113 Cl3 Fe2 P8 Pt2
Calculated formula	C149 H113 Cl3 Fe2 P8 Pt2
Title of publication	Imidazole Phosphines: Synthesis, Reaction Chemistry, and Their Use in SuzukiC,CCross-Coupling Reactions
Authors of publication	Milde, Bianca; Packheiser, Rico; Hildebrandt, Stefanie; Schaarschmidt, Dieter; Rüffer, Tobias; Lang, Heinrich
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	9
Pages of publication	3661
a	40.6012 ± 0.0007 Å
b	10.5638 ± 0.0003 Å
c	28.5311 ± 0.0006 Å
α	90°
β	98.492 ± 0.002°
γ	90°
Cell volume	12102.9 ± 0.5 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0727
Residual factor for significantly intense reflections	0.0409
Weighted residual factors for significantly intense reflections	0.089
Weighted residual factors for all reflections included in the refinement	0.098
Goodness-of-fit parameter for all reflections included in the refinement	0.884
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178721 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/32.	4083282.cif
113699	2014-05-13	cif/ Adding structures of 4083282 via cif-deposit CGI script.	4083282.cif