Crystallography Open Database

Information card for entry 4083393

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Coordinates	4083393.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	N-((dimethylamino)dimethylsilyl)-2,6-diisopropyl- benzenamino trichlorozirconium lithium
Formula	C24 H45 Cl4 Li N2 O2 Si Zr
Calculated formula	C24 H45 Cl4 Li N2 O2 Si Zr
SMILES	[Zr]12(N([Si]([N]1(C)C)(C)C)c1c(cccc1C(C)C)C(C)C)(Cl)(Cl)[Cl][Li]([Cl]2)([O]1CCCC1)[O]1CCCC1
Title of publication	μ2,η1-N-[(N,N-Dimethylamino)dimethylsilyl]-2,6-diisopropylanilido Metal (Li, Zr, Hf) Compounds and the Catalytic Behaviors of the IVB Compounds in Ethylene (Co)Polymerizationξ
Authors of publication	Yuan, Shifang; Wei, Xuehong; Tong, Hongbo; Zhang, Liping; Liu, Diansheng; Sun, Wen-Hua
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	9
Pages of publication	2085
a	9.001 ± 0.003 Å
b	10.826 ± 0.003 Å
c	19.583 ± 0.007 Å
α	104.77 ± 0.03°
β	101.15 ± 0.03°
γ	95.94 ± 0.03°
Cell volume	1786.7 ± 1.1 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0572
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.1093
Weighted residual factors for all reflections included in the refinement	0.114
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178722 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/33.	4083393.cif
114523	2014-05-24	cif/ Adding structures of 4083390, 4083391, 4083392, 4083393, 4083394, 4083395, 4083396 via cif-deposit CGI script.	4083393.cif