Crystallography Open Database

Information card for entry 4084614

Preview

Coordinates	4084614.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H95 N6 O2 Si4 Sn
Calculated formula	C65 H95 N6 O2 Si4 Sn
Title of publication	Reactivity of Tin(II) Guanidinate with 1,2- and 1,3-Diones: Oxidative Cycloaddition or Ligand Substitution ?
Authors of publication	Chlupatý, Tomáš; Růžičková, Zdeňka; Horáček, Michal; Merna, Jan; Alonso, Mercedes; De Proft, Frank; Růžička, Aleš
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	11
Pages of publication	2202
a	13.0261 ± 0.001 Å
b	13.3711 ± 0.0012 Å
c	20.8949 ± 0.001 Å
α	76.794 ± 0.006°
β	88.137 ± 0.007°
γ	73.6 ± 0.008°
Cell volume	3396.9 ± 0.5 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0644
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.0794
Weighted residual factors for all reflections included in the refinement	0.0915
Goodness-of-fit parameter for all reflections included in the refinement	1.124
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178735 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/46.	4084614.cif
140230	2015-07-05	cif/ Updating files of 4084614, 4084615, 4084616, 4084617, 4084618, 4084619 Original log message: Adding full bibliography for 4084614--4084619.cif.	4084614.cif
126103	2014-10-31	cif/ Adding structures of 4084614, 4084615, 4084616, 4084617, 4084618, 4084619 via cif-deposit CGI script.	4084614.cif