Crystallography Open Database

Information card for entry 4084624

Preview

Coordinates	4084624.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H74 N2 O2 P4 Zn2
Calculated formula	C48 H74 N2 O2 P4 Zn2
Title of publication	Structures and CO2Reactivity of Zinc Complexes of Bis(diisopropyl-) and Bis(diphenylphosphino)amines
Authors of publication	Dickie, Diane A.; Kemp, Richard A.
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	22
Pages of publication	6511
a	19.2697 ± 0.0007 Å
b	11.6675 ± 0.0005 Å
c	22.8911 ± 0.0009 Å
α	90°
β	103.908 ± 0.002°
γ	90°
Cell volume	4995.7 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0696
Residual factor for significantly intense reflections	0.0501
Weighted residual factors for significantly intense reflections	0.1206
Weighted residual factors for all reflections included in the refinement	0.1269
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178735 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/46.	4084624.cif
131431	2015-02-07	cif/ Updating files of 4084620, 4084621, 4084622, 4084623, 4084624, 4084625, 4084626, 4084627 Original log message: Adding full bibliography for 4084620--4084627.cif.	4084624.cif
126214	2014-11-04	cif/ Adding structures of 4084620, 4084621, 4084622, 4084623, 4084624, 4084625, 4084626, 4084627 via cif-deposit CGI script.	4084624.cif