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Information card for entry 4084655
Preview
Coordinates | 4084655.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C57 H49 F P3 Si |
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Calculated formula | C57 H49 F P3 Si |
Title of publication | Synthesis, Geometry, and Bonding Nature of Heptacoordinate Compounds of Silicon and Germanium Featuring Three Phosphine Donors |
Authors of publication | Kameo, Hajime; Kawamoto, Tatsuya; Sakaki, Shigeyoshi; Bourissou, Didier; Nakazawa, Hiroshi |
Journal of publication | Organometallics |
Year of publication | 2014 |
Journal volume | 33 |
Journal issue | 22 |
Pages of publication | 6557 |
a | 15.9325 ± 0.0009 Å |
b | 9.3509 ± 0.0005 Å |
c | 31.6757 ± 0.0019 Å |
α | 90° |
β | 92.601 ± 0.003° |
γ | 90° |
Cell volume | 4714.3 ± 0.5 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0993 |
Residual factor for significantly intense reflections | 0.0875 |
Weighted residual factors for significantly intense reflections | 0.1832 |
Weighted residual factors for all reflections included in the refinement | 0.1886 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.23 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
176432 (current) | 2016-02-14 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries. |
4084655.cif |
131443 | 2015-02-07 | cif/ Updating files of 4084655, 4084656, 4084657, 4084658, 4084659, 4084660 Original log message: Adding full bibliography for 4084655--4084660.cif. |
4084655.cif |
126629 | 2014-11-07 | cif/ Adding structures of 4084655, 4084656, 4084657, 4084658, 4084659, 4084660 via cif-deposit CGI script. |
4084655.cif |
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Users of the data should acknowledge the original authors of the
structural data.