Crystallography Open Database

Information card for entry 4084814

Preview

Coordinates	4084814.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H56 Al Li N2 Si4
Calculated formula	C24 H56 Al Li N2 Si4
Title of publication	Syntheses and Structures of Stable 1-Aminoalumole Derivatives
Authors of publication	Agou, Tomohiro; Wasano, Tatsuya; Sasamori, Takahiro; Tokitoh, Norihiro
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	23
Pages of publication	6963
a	17.2815 ± 0.0008 Å
b	9.8343 ± 0.0004 Å
c	18.6058 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	3162.1 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0282
Residual factor for significantly intense reflections	0.0273
Weighted residual factors for significantly intense reflections	0.0671
Weighted residual factors for all reflections included in the refinement	0.0679
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178737 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/48.	4084814.cif
131485	2015-02-08	cif/ Updating files of 4084814, 4084815 Original log message: Adding full bibliography for 4084814--4084815.cif.	4084814.cif
127748	2014-11-21	cif/ Adding structures of 4084814, 4084815 via cif-deposit CGI script.	4084814.cif