Crystallography Open Database

Information card for entry 4085563

Preview

Coordinates	4085563.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H55 Cl6 F12 N P3 Pt Sb3
Calculated formula	C63 H55 Cl6 F12 N P3 Pt Sb3
Title of publication	Guilty on Two Counts: Stepwise Coordination of Two Fluoride Anions to the Antimony Atom of a Noninnocent Stibine Ligand
Authors of publication	Jones, James S.; Wade, Casey R.; Gabba\?ï, François P.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	11
Pages of publication	2647
a	11.2596 ± 0.0015 Å
b	15.673 ± 0.002 Å
c	20.636 ± 0.003 Å
α	82.937 ± 0.002°
β	83.932 ± 0.002°
γ	70.025 ± 0.001°
Cell volume	3388.7 ± 0.8 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0732
Residual factor for significantly intense reflections	0.0657
Weighted residual factors for significantly intense reflections	0.174
Weighted residual factors for all reflections included in the refinement	0.1836
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178744 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/55.	4085563.cif
140245	2015-07-05	cif/ Updating files of 4085560, 4085561, 4085562, 4085563, 4085564 Original log message: Adding full bibliography for 4085560--4085564.cif.	4085563.cif
132446	2015-02-26	cif/ Adding structures of 4085563 via cif-deposit CGI script.	4085563.cif