Crystallography Open Database

Information card for entry 4085588

Preview

Coordinates	4085588.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	compound 2
Formula	C23 H25 P
Calculated formula	C23 H25 P
SMILES	C1(c2c(c3c1cccc3)cccc2)=P(C)(C)C.Cc1ccccc1
Title of publication	Fluorenylidene-Functionalized Lithium Phosphonium Di- and Triylides
Authors of publication	Schröder, Fabian G.; Sundermeyer, Jörg
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	6
Pages of publication	1017 - 1020
a	14.5317 ± 0.0008 Å
b	15.7241 ± 0.0006 Å
c	8.1768 ± 0.0005 Å
α	90°
β	95.232 ± 0.005°
γ	90°
Cell volume	1860.6 ± 0.17 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0873
Residual factor for significantly intense reflections	0.0406
Weighted residual factors for significantly intense reflections	0.0587
Weighted residual factors for all reflections included in the refinement	0.0659
Goodness-of-fit parameter for all reflections included in the refinement	0.806
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
209803 (current)	2018-08-16	cif/4/08/ Updating bibliography in entries 4085587-4085590, 4085648-4085651. Marking entries 4085648-4085651 as duplicates of entries 4085587-4085590.	4085588.cif
178744	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/55.	4085588.cif
134851	2015-04-04	cif/ Updating files of 4085587, 4085588, 4085589, 4085590 Original log message: Adding full bibliography for 4085587--4085590.cif.	4085588.cif
133053	2015-03-05	cif/ Adding structures of 4085587, 4085588, 4085589, 4085590 via cif-deposit CGI script.	4085588.cif