Crystallography Open Database

Information card for entry 4085630

Preview

Coordinates	4085630.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C73 H71 B2 Cl2 F8 N5 Os P2
Calculated formula	C72 H69 B2 F8 N5 Os P2
Title of publication	Bis(pyridylimino)isoindolato (BPI) Osmium Complexes: Structural Chemistry and Reactivity
Authors of publication	Müller, Astrid L.; Wadepohl, Hubert; Gade, Lutz H.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	12
Pages of publication	2810
a	12.407 ± 0.005 Å
b	15.235 ± 0.007 Å
c	18.64 ± 0.009 Å
α	108.001 ± 0.008°
β	98.002 ± 0.012°
γ	95.292 ± 0.011°
Cell volume	3284 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0386
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.0691
Weighted residual factors for all reflections included in the refinement	0.0763
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178745 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/56.	4085630.cif
140201	2015-07-05	cif/ Updating files of 4085628, 4085629, 4085630, 4085631 Original log message: Adding full bibliography for 4085628--4085631.cif.	4085630.cif
134220	2015-03-21	cif/ Adding structures of 4085628, 4085629, 4085630, 4085631 via cif-deposit CGI script.	4085630.cif