Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4085820
Preview
| Coordinates | 4085820.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38 H48 Al N5 |
|---|---|
| Calculated formula | C38 H48 Al N5 |
| Title of publication | Aluminum Alkyl Complexes Supported by Bidentate N,N Ligands: Synthesis, Structure, and Catalytic Activity for Guanylation of Amines |
| Authors of publication | Wei, Yun; Wang, Shaowu; Zhou, Shuangliu; Feng, Zhijun; Guo, Liping; Zhu, Xiancui; Mu, Xiaolong; Yao, Fangshi |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 10 |
| Pages of publication | 1882 |
| a | 9.1613 ± 0.0013 Å |
| b | 12.7665 ± 0.0018 Å |
| c | 15.639 ± 0.002 Å |
| α | 96.06 ± 0.002° |
| β | 93.002 ± 0.002° |
| γ | 101.365 ± 0.002° |
| Cell volume | 1778.2 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1295 |
| Residual factor for significantly intense reflections | 0.0584 |
| Weighted residual factors for significantly intense reflections | 0.1348 |
| Weighted residual factors for all reflections included in the refinement | 0.1679 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.993 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176428 (current) | 2016-02-13 | Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively. |
4085820.cif |
| 141374 | 2015-07-09 | cif/ Updating files of 4085814, 4085815, 4085816, 4085817, 4085818, 4085819, 4085820 Original log message: Adding full bibliography for 4085814--4085820.cif. |
4085820.cif |
| 136840 | 2015-05-18 | cif/ Adding structures of 4085814, 4085815, 4085816, 4085817, 4085818, 4085819, 4085820 via cif-deposit CGI script. |
4085820.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.