Crystallography Open Database

Information card for entry 4086030

Preview

Coordinates	4086030.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C80 H112 K2 N10 O6 Pd2
Calculated formula	C80 H112 K2 N10 O6 Pd2
Title of publication	Evidence for the Formation of Anionic Zerovalent Group 10 Complexes as Highly Reactive Intermediates
Authors of publication	Seyboldt, Alexander; Wucher, Barbara; Hohnstein, Silvia; Eichele, Klaus; Rominger, Frank; Törnroos, Karl W.; Kunz, Doris
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	12
Pages of publication	2717
a	10.6602 ± 0.0002 Å
b	16.1278 ± 0.0003 Å
c	25.0995 ± 0.0005 Å
α	90°
β	99.22 ± 0.001°
γ	90°
Cell volume	4259.49 ± 0.14 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0447
Residual factor for significantly intense reflections	0.0359
Weighted residual factors for significantly intense reflections	0.0952
Weighted residual factors for all reflections included in the refinement	0.099
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
140040 (current)	2015-07-05	cif/ Adding structures of 4086026, 4086027, 4086028, 4086029, 4086030 via cif-deposit CGI script.	4086030.cif