Crystallography Open Database

Information card for entry 4086180

Preview

Coordinates	4086180.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H48 B11 Cl11 P2 Pt Si
Calculated formula	C34 H48 B11 Cl11 P2 Pt Si
Title of publication	Silyl‒Silylene Interplay in Cationic PSiP Pincer Complexes of Platinum
Authors of publication	DeMott, Jessica C.; Gu, Weixing; McCulloch, Billy J.; Herbert, David E.; Goshert, Mitchell D.; Walensky, Justin R.; Zhou, Jia; Ozerov, Oleg V.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	16
Pages of publication	3930
a	8.8067 ± 0.001 Å
b	16.4732 ± 0.0019 Å
c	18.252 ± 0.002 Å
α	93.859 ± 0.001°
β	93.163 ± 0.001°
γ	95.343 ± 0.001°
Cell volume	2625.4 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0455
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0889
Weighted residual factors for all reflections included in the refinement	0.0935
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
211332 (current)	2018-10-05	cif/ Fixing enumeration values for CIF data items _atom_sites_solution_* using cif_fix_values. Data item relocations and exclusion of CIF comment lines might have occurred due to the usage of cif_filter.	4086180.cif
154740	2015-09-06	cif/ Updating files of 4086177, 4086178, 4086179, 4086180, 4086181 Original log message: Adding full bibliography for 4086177--4086181.cif.	4086180.cif
152947	2015-08-06	cif/ Adding structures of 4086177, 4086178, 4086179, 4086180, 4086181 via cif-deposit CGI script.	4086180.cif