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Information card for entry 4086703
Preview
| Coordinates | 4086703.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C16 H33 O4 P Rh |
|---|---|
| Calculated formula | C16 H33 O4 P Rh |
| Title of publication | Axial Tri-tert-butylphosphane Coordination to Rh2(OAc)4: Synthesis, Structure, and Catalytic Studies |
| Authors of publication | Tan, Jiantao; Kuang, Yi; Wang, Yi; Huang, Qingfei; Zhu, Jin; Wang, Yuanhua |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 18 |
| Pages of publication | 3139 |
| a | 8.8038 ± 0.0003 Å |
| b | 19.4899 ± 0.0006 Å |
| c | 12.0669 ± 0.0004 Å |
| α | 90° |
| β | 102.539 ± 0.003° |
| γ | 90° |
| Cell volume | 2021.12 ± 0.12 Å3 |
| Cell temperature | 294.39 ± 0.1 K |
| Ambient diffraction temperature | 294.39 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0696 |
| Residual factor for significantly intense reflections | 0.065 |
| Weighted residual factors for significantly intense reflections | 0.1863 |
| Weighted residual factors for all reflections included in the refinement | 0.1938 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.042 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 186935 (current) | 2016-10-05 | cif/ Adding structures of 4086703, 4086704 via cif-deposit CGI script. |
4086703.cif |
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Users of the data should acknowledge the original authors of the
structural data.