Crystallography Open Database

Information card for entry 4086952

Preview

Coordinates	4086952.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H48 K O5 P Pt S
Calculated formula	C34 H48 K O5 P Pt S
Title of publication	Facile Styrene Formation from Ethylene and a Phenylplatinum(II) Complex Leading to an Observable Platinum(II) Hydride
Authors of publication	Pal, Shrinwantu; Kusumoto, Shuhei; Nozaki, Kyoko
Journal of publication	Organometallics
Year of publication	2017
Journal volume	36
Journal issue	3
Pages of publication	502
a	11.049 ± 0.004 Å
b	13.388 ± 0.005 Å
c	23.336 ± 0.008 Å
α	90°
β	93.252 ± 0.005°
γ	90°
Cell volume	3446 ± 2 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0731
Residual factor for significantly intense reflections	0.0614
Weighted residual factors for significantly intense reflections	0.122
Weighted residual factors for all reflections included in the refinement	0.1301
Goodness-of-fit parameter for all reflections included in the refinement	1.123
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
193620 (current)	2017-03-04	cif/ Updating files of 4086950, 4086951, 4086952, 4086953 Original log message: Adding full bibliography for 4086950--4086953.cif.	4086952.cif
191041	2017-01-28	cif/ Adding structures of 4086952 via cif-deposit CGI script.	4086952.cif