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Information card for entry 4087517
Preview
| Coordinates | 4087517.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H36 O4 U |
|---|---|
| Calculated formula | C32 H36 O4 U |
| Title of publication | New Benzylpotassium Reagents and Their Utility for the Synthesis of Homoleptic Uranium(IV) Benzyl Derivatives |
| Authors of publication | Johnson, Sara A.; Kiernicki, John J.; Fanwick, Phillip E.; Bart, Suzanne C. |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 12 |
| Pages of publication | 2889 |
| a | 15.0546 ± 0.0006 Å |
| b | 12.9697 ± 0.0004 Å |
| c | 15.2621 ± 0.0004 Å |
| α | 90° |
| β | 108.171 ± 0.002° |
| γ | 90° |
| Cell volume | 2831.37 ± 0.16 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 13 |
| Hermann-Mauguin space group symbol | P 1 2/c 1 |
| Hall space group symbol | -P 2yc |
| Residual factor for all reflections | 0.0467 |
| Residual factor for significantly intense reflections | 0.0411 |
| Weighted residual factors for significantly intense reflections | 0.1205 |
| Weighted residual factors for all reflections included in the refinement | 0.1271 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.13 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 236832 (current) | 2019-11-24 | cif/ Adding structures of 4087517 via cif-deposit CGI script. |
4087517.cif |
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Users of the data should acknowledge the original authors of the
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