Crystallography Open Database

Information card for entry 4087688

Preview

Coordinates	4087688.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H20.5 Cl3 P0.5 Ru1.5
Calculated formula	C19 H20.5 Cl3 P0.5 Ru1.5
Title of publication	Synthesis and Characterization of a Family of Air-Stable Ferrocene- and Ruthenocene-Containing Primary, Secondary, and Tertiary Phosphines
Authors of publication	Kenaree, Amir Rabiee; Cuthbert, Tyler J.; Barbon, Stephanie M.; Boyle, Paul D.; Gillies, Elizabeth R.; Ragogna, Paul J.; Gilroy, Joe B.
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	17
Pages of publication	4272
a	5.778 ± 0.003 Å
b	27.701 ± 0.019 Å
c	12.417 ± 0.009 Å
α	90°
β	100.311 ± 0.017°
γ	90°
Cell volume	1955 ± 2 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0625
Residual factor for significantly intense reflections	0.0453
Weighted residual factors for significantly intense reflections	0.0847
Weighted residual factors for all reflections included in the refinement	0.0909
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
236922 (current)	2019-11-24	cif/ Adding structures of 4087687, 4087688, 4087689, 4087690, 4087691 via cif-deposit CGI script.	4087688.cif