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Information card for entry 4087759
Preview
| Coordinates | 4087759.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H31 B F4 N O2 P2 Rh |
|---|---|
| Calculated formula | C15 H31 B F4 N O2 P2 Rh |
| Title of publication | Rhodium-Catalyzed Pauson‒Khand Reaction Using a Small-Bite-Angle P-Stereogenic C1-Diphosphine Ligand |
| Authors of publication | Cristóbal-Lecina, Edgar; Costantino, Andrea R.; Grabulosa, Arnald; Riera, Antoni; Verdaguer, Xavier |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 20 |
| Pages of publication | 4989 |
| a | 8.4615 ± 0.0018 Å |
| b | 13.592 ± 0.003 Å |
| c | 19.419 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2233.4 ± 0.8 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0304 |
| Residual factor for significantly intense reflections | 0.0281 |
| Weighted residual factors for significantly intense reflections | 0.0679 |
| Weighted residual factors for all reflections included in the refinement | 0.0693 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 236989 (current) | 2019-11-24 | cif/ Adding structures of 4087759 via cif-deposit CGI script. |
4087759.cif |
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