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Information card for entry 4087929
Preview
| Coordinates | 4087929.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H36 F4 N2 Ni2 P2 S2 |
|---|---|
| Calculated formula | C30 H36 F4 N2 Ni2 P2 S2 |
| Title of publication | Imine Nitrogen Bridged Binuclear Nickel Complexes via N‒H Bond Activation: Synthesis, Characterization, Unexpected C,N-Coupling Reaction, and Their Catalytic Application in Hydrosilylation of Aldehydes |
| Authors of publication | Wang, Lin; Sun, Hongjian; Li, Xiaoyan |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 20 |
| Pages of publication | 5175 |
| a | 10.0939 ± 0.0004 Å |
| b | 31.9239 ± 0.001 Å |
| c | 10.9073 ± 0.0004 Å |
| α | 90° |
| β | 107.157 ± 0.003° |
| γ | 90° |
| Cell volume | 3358.3 ± 0.2 Å3 |
| Cell temperature | 150.15 K |
| Ambient diffraction temperature | 150.15 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0296 |
| Residual factor for significantly intense reflections | 0.0285 |
| Weighted residual factors for significantly intense reflections | 0.071 |
| Weighted residual factors for all reflections included in the refinement | 0.0715 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237131 (current) | 2019-11-24 | cif/ Adding structures of 4087928, 4087929, 4087930 via cif-deposit CGI script. |
4087929.cif |
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Users of the data should acknowledge the original authors of the
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