Crystallography Open Database

Information card for entry 4087939

Preview

Coordinates	4087939.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H41 Au Cl N3 Si3
Calculated formula	C21 H41 Au Cl N3 Si3
SMILES	[Au](Cl)[Si]1(N([Si](C)(C)C)[Si](C)(C)C)[N](C(C)(C)C)=C(c2ccccc2)N1C(C)(C)C
Title of publication	Silicon(II) Bis(trimethylsilyl)amide (LSiN(SiMe3)2, L = PhC(NtBu)2) Supported Copper, Silver, and Gold Complexes
Authors of publication	Khan, Shabana; Ahirwar, Saurabh K.; Pal, Shiv; Parvin, Nasrina; Kathewad, Neha
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	22
Pages of publication	5401
a	8.904 ± 0.003 Å
b	18.36 ± 0.007 Å
c	17.794 ± 0.007 Å
α	90°
β	101.464 ± 0.009°
γ	90°
Cell volume	2850.9 ± 1.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0281
Residual factor for significantly intense reflections	0.021
Weighted residual factors for significantly intense reflections	0.0452
Weighted residual factors for all reflections included in the refinement	0.0502
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
237142 (current)	2019-11-24	cif/ Adding structures of 4087939 via cif-deposit CGI script.	4087939.cif