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Information card for entry 4087982
Preview
| Coordinates | 4087982.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C103 H126 Mo2 N8 O10 P2 Si2 |
|---|---|
| Calculated formula | C103 H126 Mo2 N8 O10 P2 Si2 |
| Title of publication | Transition Metal Complexes of a “Half-Parent” Phosphasilene Adduct Representing Silylene→Phosphinidene→Metal Complexes |
| Authors of publication | Hansen, Kerstin; Szilvási, Tibor; Blom, Burgert; Driess, Matthias |
| Journal of publication | Organometallics |
| Year of publication | 2015 |
| Journal volume | 34 |
| Journal issue | 24 |
| Pages of publication | 5703 |
| a | 15.9982 ± 0.0013 Å |
| b | 20.0928 ± 0.0008 Å |
| c | 17.7845 ± 0.001 Å |
| α | 90° |
| β | 114.755 ± 0.009° |
| γ | 90° |
| Cell volume | 5191.5 ± 0.7 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 0.1 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1237 |
| Residual factor for significantly intense reflections | 0.0741 |
| Weighted residual factors for significantly intense reflections | 0.1612 |
| Weighted residual factors for all reflections included in the refinement | 0.1936 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237172 (current) | 2019-11-24 | cif/ Adding structures of 4087982 via cif-deposit CGI script. |
4087982.cif |
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