Crystallography Open Database

Information card for entry 4088061

Preview

Coordinates	4088061.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	2,2,-Bis{bis[bis(trimethylsilyl)methyl-chlorido-stannyl]}propane
Formula	C32.5 H85 Cl2 O0.5 Si8 Sn2
Calculated formula	C31 H82 Cl2 Si8 Sn2
Title of publication	Cyclic Dinuclear Organotin Cations Stabilized by Bulky Substituents
Authors of publication	Wagner, Michael; Zobel, Bernhard; Dietz, Christina; Schollmeyer, Dieter; Jurkschat, Klaus
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	23
Pages of publication	5602
a	28.4631 ± 0.001 Å
b	23.2026 ± 0.0005 Å
c	16.3645 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	10807.4 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.077
Residual factor for significantly intense reflections	0.0483
Weighted residual factors for significantly intense reflections	0.1331
Weighted residual factors for all reflections included in the refinement	0.1477
Goodness-of-fit parameter for all reflections included in the refinement	0.96
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237238 (current)	2019-11-24	cif/ Adding structures of 4088061, 4088062, 4088063, 4088064, 4088065 via cif-deposit CGI script.	4088061.cif