Crystallography Open Database

Information card for entry 4088065

Preview

Coordinates	4088065.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	'[1,1,3,3-bistrimethylsilylmethyl,4,4-dimethyl]-2-oxo-1,3-distannetane'
Formula	C31 H82 O Si8 Sn2
Calculated formula	C31 H82 O Si8 Sn2
Title of publication	Cyclic Dinuclear Organotin Cations Stabilized by Bulky Substituents
Authors of publication	Wagner, Michael; Zobel, Bernhard; Dietz, Christina; Schollmeyer, Dieter; Jurkschat, Klaus
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	23
Pages of publication	5602
a	21.8 ± 0.006 Å
b	9.497 ± 0.0004 Å
c	25.406 ± 0.003 Å
α	90°
β	106.313 ± 0.015°
γ	90°
Cell volume	5048.2 ± 1.6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0849
Residual factor for significantly intense reflections	0.0807
Weighted residual factors for significantly intense reflections	0.2192
Weighted residual factors for all reflections included in the refinement	0.2277
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237238 (current)	2019-11-24	cif/ Adding structures of 4088061, 4088062, 4088063, 4088064, 4088065 via cif-deposit CGI script.	4088065.cif